المصدر: Sample Preparation in Chromatography في منتدى : قسم الكيمياء بسم الله الرحمن الرحيم Sample Preparation in Chromatography Publisher: Elsevier Science Number Of Pages: 942 Publication Date: 2002-05-01 Sales Rank: 2087047 ISBN / ASIN: 0444503943 EAN: 9780444503947 Binding: Hardcover Manufacturer: Elsevier Science Studio: Elsevier Science Book Description: Sample preparation is an essential step in many analyses. This book approaches the topic of sample preparation in chromatography in a methodical way, viewing it as a logical connection between sample collection and analytical chromatography. Providing a guide for choosing the appropriate sample preparation for a given analysis, this book describes various ways to process the sample, explaining the principle, discussing the advantages and disadvantages, describing the applicability to different types of samples, and showing the fitness to specific chromatographic determinations. The first part of the book contains an overview of sample preparation showing its relation to sample collection and to the core chromatographic analysis. The second part covers procedures that do not use chemical modifications of the analyte and includes methods for sample dissolution, concentration and cleanup designed mainly for modifying the initial matrix of the sample. This part starts with conventional separations such as filtration and distillation and finishes with more advanced techniques such as solid phase extraction and electroseparations. The third part gives a description of the chemical modifications that can be performed on a sample either for fractionation purposes or to improve a specific property of the analyte. This part includes derivatizations, polymer chemical degradations, and pyrolysis. الروابط في المرفقات وتقبلوا تحياتي
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