"Experimental Organic Chemistry: A Miniscale and Microscale Approach" by John C. Gilbert, Stephen F. Martin
|
"Experimental Organic Chemistry: A Miniscale and Microscale Approach" by John C. Gilbert, Stephen F. Martin
Fifth Edition
Brooks/Cole, Cengage Learning | 2011 | ISBN: 1439049149 9781111385712 9781439049143 | 966 pages | PDF | 54 MB
This edition contains procedures for both miniscale (also known as small scale) and microscale users. The manual first provides an early focus on equipment, record keeping, and safety in the laboratory, then walks students step by step through the laboratory techniques they need to perform the book's experiments with confidence.
Chapters show students how to use the book's techniques to synthesize compounds and analyze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds.
A bioorganic experiment in 24 reflects the increasing emphasis on bioorganic chemistry in the course and gives students an opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide.
Contents in Brief
Equipment Commonly Used in the Organic Chemistry Laboratory
First Aid in Case of an Accident
Discovery Experiments
Periodic Table of the Elements
Approximate 1H and 13C NMR Shifts
Experimental Organic Chemistry: A Miniscale and Microscale Approach
Table of Contents
Preface
1 Introduction, Record Keeping, and Laboratory Safety
2 Techniques and Apparatus
3 Solids: Recrystallization and Melting Points
4 Liquids: Distillation and Boiling Points
5 Extraction
6 Chromatography
7 Stereoisomers
8 Spectral Methods
9 Alkanes
10 Alkenes
11 Alkynes
12 Dienes: The Die Is-Alder Reaction
13 Kinetic and Thermodynamic Control of a Reaction
14 Nucleophilic Aliphatic Substitution: Preparation of Alkyl Halides
15 Electrophilic Aromatic Substitution
16 Oxidation of Alcohols and Carbonyl Compounds
17 Reduction Reactions of Double Bonds: Alkenes, Carbonyl Compounds, and Imines
18 Reactions of Carbonyl Compounds
19 Organo metal lie Chemistry
20 Car boxy lie Acids and Their Derivatives
21 Multistep Organic Synthesis
22 Polymers
23 Carbohydrates
24 a-Amino Acids and Peptides
25 Identifying Organic Compounds
26 The Literature of Organic Chemistry
Index
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|
"Experimental Organic Chemistry: A Miniscale and Microscale Approach" by John C. Gilbert, Stephen F. Martin
Fifth Edition
Brooks/Cole, Cengage Learning | 2011 | ISBN: 1439049149 9781111385712 9781439049143 | 966 pages | PDF | 54 MB
This edition contains procedures for both miniscale (also known as small scale) and microscale users. The manual first provides an early focus on equipment, record keeping, and safety in the laboratory, then walks students step by step through the laboratory techniques they need to perform the book's experiments with confidence.
Chapters show students how to use the book's techniques to synthesize compounds and analyze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds.
A bioorganic experiment in 24 reflects the increasing emphasis on bioorganic chemistry in the course and gives students an opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide.
Contents in Brief
Equipment Commonly Used in the Organic Chemistry Laboratory
First Aid in Case of an Accident
Discovery Experiments
Periodic Table of the Elements
Approximate 1H and 13C NMR Shifts
Experimental Organic Chemistry: A Miniscale and Microscale Approach
Table of Contents
Preface
1 Introduction, Record Keeping, and Laboratory Safety
2 Techniques and Apparatus
3 Solids: Recrystallization and Melting Points
4 Liquids: Distillation and Boiling Points
5 Extraction
6 Chromatography
7 Stereoisomers
8 Spectral Methods
9 Alkanes
10 Alkenes
11 Alkynes
12 Dienes: The Die Is-Alder Reaction
13 Kinetic and Thermodynamic Control of a Reaction
14 Nucleophilic Aliphatic Substitution: Preparation of Alkyl Halides
15 Electrophilic Aromatic Substitution
16 Oxidation of Alcohols and Carbonyl Compounds
17 Reduction Reactions of Double Bonds: Alkenes, Carbonyl Compounds, and Imines
18 Reactions of Carbonyl Compounds
19 Organo metal lie Chemistry
20 Car boxy lie Acids and Their Derivatives
21 Multistep Organic Synthesis
22 Polymers
23 Carbohydrates
24 a-Amino Acids and Peptides
25 Identifying Organic Compounds
26 The Literature of Organic Chemistry
Index
[HIDE]
DepositF • | • RGator
UlNet • | • SiBi • | • TuBi[/HIDE]
