المصدر: كتاب : Experimental Organic Chemistry: A Miniscale and Microscale Approach في منتدى : قسم الكيمياء "Experimental Organic Chemistry: A Miniscale and Microscale Approach" by John C. Gilbert, Stephen F. Martin | "Experimental Organic Chemistry: A Miniscale and Microscale Approach" by John C. Gilbert, Stephen F. Martin Fifth Edition Brooks/Cole, Cengage Learning | 2011 | ISBN: 1439049149 9781111385712 9781439049143 | 966 pages | PDF | 54 MB This edition contains procedures for both miniscale (also known as small scale) and microscale users. The manual first provides an early focus on equipment, record keeping, and safety in the laboratory, then walks students step by step through the laboratory techniques they need to perform the book's experiments with confidence. Chapters show students how to use the book's techniques to synthesize compounds and analyze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds. A bioorganic experiment in 24 reflects the increasing emphasis on bioorganic chemistry in the course and gives students an opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide. Contents in Brief Equipment Commonly Used in the Organic Chemistry Laboratory First Aid in Case of an Accident Discovery Experiments Periodic Table of the Elements Approximate 1H and 13C NMR Shifts Experimental Organic Chemistry: A Miniscale and Microscale Approach Table of Contents Preface 1 Introduction, Record Keeping, and Laboratory Safety 2 Techniques and Apparatus 3 Solids: Recrystallization and Melting Points 4 Liquids: Distillation and Boiling Points 5 Extraction 6 Chromatography 7 Stereoisomers 8 Spectral Methods 9 Alkanes 10 Alkenes 11 Alkynes 12 Dienes: The Die Is-Alder Reaction 13 Kinetic and Thermodynamic Control of a Reaction 14 Nucleophilic Aliphatic Substitution: Preparation of Alkyl Halides 15 Electrophilic Aromatic Substitution 16 Oxidation of Alcohols and Carbonyl Compounds 17 Reduction Reactions of Double Bonds: Alkenes, Carbonyl Compounds, and Imines 18 Reactions of Carbonyl Compounds 19 Organo metal lie Chemistry 20 Car boxy lie Acids and Their Derivatives 21 Multistep Organic Synthesis 22 Polymers 23 Carbohydrates 24 a-Amino Acids and Peptides 25 Identifying Organic Compounds 26 The Literature of Organic Chemistry Index هذا المحتوى يظهر للاعضاء المسجلين فقط: هذا المحتوى يظهر للاعضاء المسجلين فقط:
