كيمياء تحليلية كتاب Modern Derivatization Methods for Separation Sciences - Toshimasa Toyo'oka

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    كتاب طلبه أحد الأخوة الأعضاء :

    Modern Derivatization Methods for Separation Sciences - Toshimasa Toyo'oka

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    Product Details

    Hardcover: 588 pages pdf
    Publisher: Wiley (March 31, 1999)
    Language: English
    ISBN-10: 0471983640
    ISBN-13: 978-0471983644

    Editorial Reviews

    Review :
    "The methodologies suggested in this book are very useful in the life science...It is highly recommended for biochemists, separation scientists as well as postgraduate researches in these areas."

    Table of contents :

    1.Pretreatment for Real Sample Analysis and Choice of Suitable Reagent.
    (1.1) Derivatization for Drugs; Introduction; Application of Derivatization of Drugs; Determination of Pravastatin Sodium in Plasma by HPLC with laser-induced fluorescence detection after immobilized antibody extraction; enantiometric determination of ibuprofen in rat plasma using chiral fluorescence derivatization reagent; specific fluorogenic derivatization of ivermectin using non-fluorescent reagents; other methods; conclusion; references.

    (1.2) Derivatization of Agrochemicals; Introduction; Sample preparation; Derivatization in Food Analysis; Analysis of Nutrients; Carbohydrates; Amino acids and peptides; Fatty acids; Organic acids; Vitamins; Minerals; Analysis of Food Additives; Preservatives; Antioxidants; Sweeteners; Emulsifiers; Other food additives; Analysis of Veterinary Medicine; Sulfonamides; Antibiotics; Antiparasitic Agents; Analysis of pesticides; Analysis of natural toxins; mycotoxins; marine toxins; plant toxin; Analysis of food contaminants; Amines; Organotin; Hydroperoxides; Isocyanate monomers; References.

    (1.3) Derivatization for environmental contaminants; Introduction; environmental samples; gas sample; Soil and various water samples; Application; Aldehydes and ketones in air; Aliphatic amines in air; Residual pesticides and herbicides in soil and water; References.

    (2) Reagent for UV-VIS detection; Introduction; Label of amines and amino acids; Nitrobenzenes; Acetic anhydride; Isocyanates and Isothiocyanates; Acyl Chlorides; Ninhydrin; Diethylethoxymethylenemalonate (DEMM); AQC; Disuccinimido carbonate (DSC); Sold-phase reagent with UV or VIS Light Absorbing Moiety; Polymeric 3,5- Dintrobenzoyl tagged derivatization reagent; Polymeric 6-Aminoquinoline tagged derivatization reagent; Polymeric benzotriazole activated reagent containing FMOC group.

    (2.3) Label of carboxyl (-COOH); Alkyl halides; aromatic amines; Hydrazines; hydroxylamine.

    (2.4) Label of hydroxyl (-OH0; acyl halides; acid anhydrides; isocyanates; other reagents.

    (2.5) Label of reducing carbohydrate; Reductive amination; 1-Phenyl-3-methyl-5-pyrazolone; Post-column derivatization reagent.

    (2.6) Label of thiol (-SH); 2-Halopyridinium Salt; Disulfide Reagent; Other reagents.

    (2.7) Labelling of other compounds; 1-(2-Pyridyl)-piperazine (PYP); Diethyldithiocarbamate (DDTC); 9-Methylamino-methylanthracene (MAMA); References.

    (3) Reagent for FL Detection; Abbreviations; Introduction; reagents for amines and amino acids; General amino compounds; Primary amines and amino acids; Primary and secondary amines and amino acids; Particular amines and amino acids; Catecholamines; Tryptophan and indolamines; 5-hydroxyindoleamines (serotonin related compounds); Guanidino compounds; Peptides; Genral peptides; Arginine-containing peptides; Fluorescence derivatization for CE.

    (3.3) Reagents for organic acids; Carboxylic acids; Fatty acids; Prostaglandnis; Steroids; Glucuronic acid conjugates; Alpha-keto acids; Sialic acids and dehydroascorbic acids.

    (3.4) Reagents for alcohols.

    (3.5) Reagents for phenols.

    (3.6) reagents for thiols.

    (3.7) Reagents for aldehydes and ketones.

    (3.8) Reagents for carbohydrates.

    (3.9) reagents for dienes.

    (3.10) Reagents for nucleic acids related compounds.

    References.

    (4) Reagents for CL detection.

    (4.1) Introduction.

    (4.2) Label of amines.

    (4.3) Label of carboxy.

    (4.4) Label of hydroxyl and thiol.

    (4.5) Label of other functional groups.

    (4.6) Applications.

    References.

    (5) Reagents for electrochemical detection.

    (5.1) Introduction; Amperometric analysis in flowing streams; electrochemical detectors; electrode material; electrode configuration; mobile phase; chemical derivatization.

    (5.2) Labeling of primary and secondary amines; 0-phthalaldehyde; naphthalene-2,3-dicarbaldehyde; ferrocene; isocyanate and isothiocyanate; salicylic acid chloride; 2,4-Dintrofluorobenzene; 1,2-Diphenylethylenediamine; Bolton and Hunter type reagent; Others.

    (5.3) Labeling of carboxy groups.

    (5.4) Labeling of hydroxy groups.

    (5.5) Labeling of thiol groups.

    (5.6) Labeling of other functional groups.

    (5.7) Applications.

    References.

    (6) Derivatization for resolution of chiral compounds.

    (6.1) Introduction; Fundamentals of stereochemistry; Chirality and biological activity; Chirality application as single isomers.

    (6.2) Resolution of racemates; direct resoltuion; indirect resolution.

    (6.3) Reactions of various functional groups; amines; Carboxyls; Hydroxyls; Thiols and others.

    (6.4) Derivatization for LC analysis; label for alcohols; label for carboxylic acids; label for aldehydes and ketones; label for other functional groups.

    (6.5) Derivatization for LC analysis; label for UV-VIS detection; label for primary and secondary amines; label for carboxylic acids; label for alcohols; label for other functional groups; label for fluorescence (FL), laser-induced fluorescence (LIF) and chemiluminescence (CL) detection; label for primary and secondary amines including amino acids; label for carboxylic acids; label for alcohols; label for aldehydes and ketones; label for thiols; label for other functional groups; derivatization for electrochemical (EC) detection.

    (6.6) Derivatization for capillary electrophoresis (CE) analysis.

    (6.7) Conclusion and further perspective;

    References.

    Subject index.

    5.04 ميجا
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