بسم الله الرحمن الرحيم
Infrared Spectroscopy in Conservation Science
(Scientific Tools for Conservation Series)
By
Michele R. Derrick, Dusan C. Stulik, James M. Landry
Publisher
Getty Publications
Number Of Pages: 248
Publication Date: 2000-03-16
ISBN-10 / ASIN: 0892364696
ISBN-13 / EAN: 9780892364695
Product Description
This book provides practical information on the use of infrared spectroscopy for the analysis of materials found in cultural objects. Designed for scientists and students in the fields of archaeology, art conservation, microscopy, forensics, chemistry, and optics, the book discusses techniques for examining the microscopic amounts of complex, aged components in objects such as paintings, sculptures, and archaeological fragments.
Contents
Cover
Title Page
Copyright
Contents
Foreword
Preface
Acknowledgments
Chapter 1: History of Infrared Spectroscopy
Additional Reading
Chapter 2: Infrared Absorption Theory
Electromagnetic Radiation
Absorption Theory
Infrared Spectra
Infrared Regions
Near-infrared region
Mid-infrared region
Far-infrared region
Summary
Additional Reading
Chapter 3: Sample Collection and Preparation
Sampling Methodology
Sampling Implementation
Tools
Sample documentation and storage
Avoidance of contamination
Sample Collection and Preparation Procedures
Gases
Liquids
Sampling with swabs
Solids, powders, and particles
Mixture separation by solvent extractions
Mixture separation by pyrolysis
Fibers
Cross sections
Embedding media and procedures
Microtoming procedures
Summary
Additional Reading
Chapter 4: Infrared Analysis Methods
Infrared Transmission Measurements
Infrared window materials
Transmission analysis of gases
Transmission analysis of liquids
Transmission analysis of solids
Pellets and micropellets
Unsupported films
Films on diamond cells
Fiber
Infrared Reflection Measurements
Specular reflection
Reflection-absorption
Diffuse reflection
Internal reflection
Infrared Microspectroscopy
Microspectrophotometer design
Microspectrophotometer capabilities
Particle and fiber analysis
Cross section analysis
Mapping studies
Microspectrophotometer accessories
Summary
Additional Reading
Chapter 5: Spectral Interpretation
Infrared Spectra
Absorption bands
Band frequency
Band shape
Band intensity
Instrument configuration
Qualitative Analysis
Spectral quality
Visual comparison
Computer libraries
Spectral region examination
Spectra-structure correlations
Correlation charts
Identification of Materials Used in Art and Art Conservation
Natural organic materials
Flowchart for natural organic materials
Waxes
Oils
Resins (tree)
Resins (insect)
Gums
Synthetic resins (polymers)
Flowchart for synthetic resins
Characterization process for polymers
Colorants
Characterization process for pigments
Infrared spectral characterization of pigments
Mixtures
Quantitative Analysis
Mathematical Manipulations of Spectra
Subtraction techniques
Resolution enhancement methods
Summary
Additional Reading
Chapter 6: Case Studies
Identification and Characterization of Materials
Deterioration Studies
The Case Studies
Case Study 1: Ultramarine Pigments
Background
Analysis question
Method
Analysis
Results
Resolution
Case Study 2: Creosote Lac Resin
Case Study 3: Chumash Indian Paints
Case Study 4: Varnish on a Desk
Case Study 5: Reflection versus Transmission
Case Study 6: Painting Cross Sections
Case Study 7: Vikane
Case Study 8: Parylene
Case Study 9: Cellulose Nitrate Sculptures
Case Study 10: Dead Sea Scrolls
Summary
Appendix I: Selected Infrared Spectra Collections andDigitized Libraries
Appendix II: Infrared Reference Spectra
Gum Arabic
Gum Tragacanth
Rice Starch
Honey, Clover
Hide Glue
Isinglass
Gelatin
Casein
Egg Yolk, Hen
Microcrystalline Wax
Beeswax, Crude
Carnauba Wax
Linseed Stand Oil
Poppyseed Oil
Walnut Oil
Rosin
Pine Resin
Copal, Manila
Dammar
Resin Elemi
Resin
Mastic
Sandarac
Shellac
Cellulose Nitrate
Acryloid
Polyester
Poly(vinyl acetate)(PVAC)
BEVA
Polycyclohexanone
Polyamide
Chalk:
Gypsum:
Plaster:
Silica :
Barium Sulfate :
Phthalocyanine Blue
Malachite:
Madder
Dragon's Blood
Glossary
Suppliers
References
Index
About the Authors
LinK
http://ifile.it/dwtnp4j/_0892364696.rar
Infrared Spectroscopy in Conservation Science
(Scientific Tools for Conservation Series)
By
Michele R. Derrick, Dusan C. Stulik, James M. Landry
Publisher
Getty Publications
Number Of Pages: 248
Publication Date: 2000-03-16
ISBN-10 / ASIN: 0892364696
ISBN-13 / EAN: 9780892364695
Product Description
This book provides practical information on the use of infrared spectroscopy for the analysis of materials found in cultural objects. Designed for scientists and students in the fields of archaeology, art conservation, microscopy, forensics, chemistry, and optics, the book discusses techniques for examining the microscopic amounts of complex, aged components in objects such as paintings, sculptures, and archaeological fragments.
Contents
Cover
Title Page
Copyright
Contents
Foreword
Preface
Acknowledgments
Chapter 1: History of Infrared Spectroscopy
Additional Reading
Chapter 2: Infrared Absorption Theory
Electromagnetic Radiation
Absorption Theory
Infrared Spectra
Infrared Regions
Near-infrared region
Mid-infrared region
Far-infrared region
Summary
Additional Reading
Chapter 3: Sample Collection and Preparation
Sampling Methodology
Sampling Implementation
Tools
Sample documentation and storage
Avoidance of contamination
Sample Collection and Preparation Procedures
Gases
Liquids
Sampling with swabs
Solids, powders, and particles
Mixture separation by solvent extractions
Mixture separation by pyrolysis
Fibers
Cross sections
Embedding media and procedures
Microtoming procedures
Summary
Additional Reading
Chapter 4: Infrared Analysis Methods
Infrared Transmission Measurements
Infrared window materials
Transmission analysis of gases
Transmission analysis of liquids
Transmission analysis of solids
Pellets and micropellets
Unsupported films
Films on diamond cells
Fiber
Infrared Reflection Measurements
Specular reflection
Reflection-absorption
Diffuse reflection
Internal reflection
Infrared Microspectroscopy
Microspectrophotometer design
Microspectrophotometer capabilities
Particle and fiber analysis
Cross section analysis
Mapping studies
Microspectrophotometer accessories
Summary
Additional Reading
Chapter 5: Spectral Interpretation
Infrared Spectra
Absorption bands
Band frequency
Band shape
Band intensity
Instrument configuration
Qualitative Analysis
Spectral quality
Visual comparison
Computer libraries
Spectral region examination
Spectra-structure correlations
Correlation charts
Identification of Materials Used in Art and Art Conservation
Natural organic materials
Flowchart for natural organic materials
Waxes
Oils
Resins (tree)
Resins (insect)
Gums
Synthetic resins (polymers)
Flowchart for synthetic resins
Characterization process for polymers
Colorants
Characterization process for pigments
Infrared spectral characterization of pigments
Mixtures
Quantitative Analysis
Mathematical Manipulations of Spectra
Subtraction techniques
Resolution enhancement methods
Summary
Additional Reading
Chapter 6: Case Studies
Identification and Characterization of Materials
Deterioration Studies
The Case Studies
Case Study 1: Ultramarine Pigments
Background
Analysis question
Method
Analysis
Results
Resolution
Case Study 2: Creosote Lac Resin
Case Study 3: Chumash Indian Paints
Case Study 4: Varnish on a Desk
Case Study 5: Reflection versus Transmission
Case Study 6: Painting Cross Sections
Case Study 7: Vikane
Case Study 8: Parylene
Case Study 9: Cellulose Nitrate Sculptures
Case Study 10: Dead Sea Scrolls
Summary
Appendix I: Selected Infrared Spectra Collections andDigitized Libraries
Appendix II: Infrared Reference Spectra
Gum Arabic
Gum Tragacanth
Rice Starch
Honey, Clover
Hide Glue
Isinglass
Gelatin
Casein
Egg Yolk, Hen
Microcrystalline Wax
Beeswax, Crude
Carnauba Wax
Linseed Stand Oil
Poppyseed Oil
Walnut Oil
Rosin
Pine Resin
Copal, Manila
Dammar
Resin Elemi
Resin
Mastic
Sandarac
Shellac
Cellulose Nitrate
Acryloid
Polyester
Poly(vinyl acetate)(PVAC)
BEVA
Polycyclohexanone
Polyamide
Chalk:
Gypsum:
Plaster:
Silica :
Barium Sulfate :
Phthalocyanine Blue
Malachite:
Madder
Dragon's Blood
Glossary
Suppliers
References
Index
About the Authors
LinK
http://ifile.it/dwtnp4j/_0892364696.rar