كيمياء تحليلية Books on Thermal Analysis

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Some Books on Thermal Analysis

Handbook of Thermal Analysis


By T. Hatakeyama,
Publisher Wiley
Publication date March 19, 1999
Number of pages 470 pages
Book Description
Handbook of Thermal Analysis Edited by T. Hatakeyama National Institute of Materials and Chemical Research, Ibaraki, Japan Zhenhai Liu Changchun Institute of Applied Chemistry, China This book covers a comprehensive description of the principles of thermal analysis (TA) instruments, operating conditions, and the nature of the experimental data. Presented in a compact and well-arranged style with a large number of figures and illustrations, this work is divided into two parts. Part I is designed to acquaint and orient newcomers with TA by providing a comprehensive introduction to the basic principles of instrument operation, with advice on sample preparation and optimization of operating conditions, and a guide to interpreting results. The text deals primarily with techniques such as differential scanning calorimetry (DSC), differential thermal analysis (DTA), and thermogravimetry (TG). Part II illustrates 500 TA curves covering metals, inorganic and organic minerals, polymers, construction materials, pharmaceuticals, explosives, etc. The appendices include a glossary of TA terms, a survey of reference materials, the current table of TA standards, and a TA database.


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Introduction to Thermal Analysis: Techniques and Applications (Hot Topics in Thermal Analysis and Calorimetry)


By M.E. Brown
Publisher: Springer
Number of Pages: 280
Publication Date: 2001-12-31
Book Description:
Thermal Analysis is a well-established set of techniques for obtaining qualitative and quantitative information about the effects of various heat treatments on materials of all kinds, including new chemical compounds, plastics, ceramics, alloys, construction materials, minerals, foods and medicines. Heating is performed under strictly controlled conditions and can reveal changes in structure and other important properties of the material being studied. Such studies are of great practical importance in the use of materials. This new edition has been thoroughly revised and rewritten to account for the changes that have occurred in the techniques and the instrumentation since the original edition in 1988. These changes include the introduction of new modulated temperature techniques and the exciting world of micro thermal analysis, based on novel adaptations of atomic force microscopy. These new techniques are integrated with the older standard techniques. The aim of the original edition has, however, been retained and is to provide a brief, readable introduction to these versatile techniques, for anyone contemplating their use, from which it is possible to move on to the specialist literature.
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Principles of Thermal Analysis and Calorimetry



By P.J. Haines
Publisher: Royal Society of Chemistry
Number of Pages: 320
Publication Date: 2002-05-31
Book Description:
The use of thermal and calorimetric methods has shown rapid growth over the last two decades, in an increasingly wide range of applications. In addition, a number of powerful new techniques have been developed. This book supplies a concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Brief accounts of the basic theory are reinforced with detailed applications of the methods and contemporary developments. Also included is information on standard test methods and manufacturers. Written by acknowledged experts, "Principles of Thermal Analysis and Calorimetry" is up-to-date, wide-ranging and practical. It will be an important source of information for many levels of readership in a variety of areas, from students and lecturers to industrial and laboratory staff and consultants.
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Principles and Applications of Thermal Analysis


By Paul Gabbott
Publisher: Wiley-Blackwell
Number of Pages: 480
Publication Date: 2007-11-16
Book Description:
Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides sound practical instruction on using the techniques and gives an up-to-date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then discussing industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues, the book serves as an important reference for experienced analysts.
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Introduction to Thermal Analysis

By M.E. Brown
Publisher: Springer
Number of Pages: 224
Publication Date: 1988-06-30
Book Description:
Thermal Analysis is a well-established set of techniques for obtaining qualitative and quantitative information about the effects of various heat treatments on materials of all kinds, including new chemical compounds, plastics, ceramics, alloys, construction materials, minerals, foods and medicines. Heating is performed under strictly controlled conditions and can reveal changes in structure and other important properties of the material being studied. Such studies are of great practical importance in the use of materials.
This new edition has been thoroughly revised and rewritten to account for the changes that have occurred in the techniques and the instrumentation since the original edition in 1988. These changes include the introduction of new modulated temperature techniques and the exciting world of micro thermal analysis, based on novel adaptations of atomic force microscopy. These new techniques are integrated with the older standard techniques.
The aim of the original edition has, however, been retained and is to provide a brief, readable introduction to these versatile techniques, for anyone contemplating their use, from which it is possible to move on to the specialist literature.
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Thermal analysis 3rd edition


By Wesley Wm. Wendlandt
Publisher: Wiley-Interscience
Number of Pages: 832
Publication Date: 1986-02-24
Book Description:
Provides a comprehensive introduction to thermal analysis and its usefulness in every area of science from archeology to zoology. Covers many new applications of techniques in TG, DTA, DSC, EGD/EGA, and others. Describes instruments available for each technique, including microcomputers. Includes rewritten chapters on EGD/EGA, miscellaneous techniques, and the determination of purity by DSC.

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Handbook of Thermal Analysis and Calorimetry:
By Michael E. Brown
Publisher: Elsevier Science






Volume 1 Principles and Practice
Number of Pages: 722
Publication Date: 1998-09-01
Book Description:
Volume 1 describes the basic background information common to thermal analysis and calorimetry in general. Thermodynamic and kinetic principles are discussed along with the instrumentation and methodology associated with thermoanalytical and calorimetric techniques. The purpose is to collect the discussion of these general principles and minimize redundancies in the subsequent volumes that are concerned with the applications of these principles and methods. More unique methods, which pertain to specific processes or materials, are covered in later volumes.

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Volume 2: Applications to inorganic and miscellaneous materials
Number of Pages: 942
Publication Date: 2003-12-08
Book Description:
This is the second volume of a four volume set intended to describe the techniques and applications of thermoanalytical and calorimetric methods. The general techniques and methodology are covered extensively in Volume 1, along with the fundamental physicochemical background needed. Consequently the subsequent volumes dwell on the applications of these powerful and versatile methods, while assuming a familiarity with the techniques.
Volume 2 covers major areas of inorganic materials and some related general topics, e.g., catalysis, geochemistry, and the preservation of art. The chapters are written by established practitioners in the field with the intent of presenting a sampling of the how thermoanalytical and calorimetric methods have contributed to progress in their respective areas. The chapters are not intended as exhaustive reviews of the topics, but rather, to illustrate to the readers what has been achieved and to encourage them to consider extending these applications further into their domains of interest

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Volume 3 Applications to Polymers and Plastics
Number of Pages: 850
Publication Date: 2002-12-01
Book Description:
As a new and exciting field of interdisciplinary macromolecular science and engineering, polymeric materials will have a profound presence in 21st century chemical, pharmaceutical, biomedical, manufacturing, infrastructure, electronic, optical and information technologies. The origin of this field derived from an area of polymer science and engineering encompassing plastic technologies. The field is rapidly expanding to incorporate new interdisciplinary research areas such as biomaterials, macromolecular biology, novel macromolecular structures, environmental macromolecular science and engineering, innovative and nano-fabrications of products, and is translating discoveries into technologies.


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Volume 4 from Macromolecules to Man
Number of Pages1060
Publication Date: 1999-12-01
Book Description:
The applications and interest in thermal analysis and calorimetry have grown enormously during the last half of the 20th century. These techniques have become indispensable in the study of processes such as catalysis, hazards evaluation etc., and in measuring important physical properties quickly, conveniently and with markedly improved accuracy. Consequently, thermal analysis and calorimetry have grown in stature and more scientists and engineers have become at least part-time, practitioners. People new to the field therefore need a source of information describing the basic principles and current state of the art. The last volume of this 4 volume handbook, devoted to many aspects of biological thermal analysis and calorimetry, completes a comprehensive review of this important area. All chapters have been prepared by recognized experts in their respective fields. The approach taken is "how and what to do and when to do it". The complete work is a valuable addition to the already existing literature.

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Volume 5 Volume 5: Recent Advances, Techniques and Applications
Number of Pages: 780
Publication Date: 2007-12-17
Book Description:
This is Volume 5 of a Handbook that has been well-received by the thermal analysis and calorimetry community. All chapters in all five volumes are written by international experts in the subject. The fifth volume covers recent advances in techniques and applications that complement the earlier volumes. The chapters refer wherever possible to earlier volumes, but each is complete in itself. The latest recommendations on Nomenclature are also included. Amongst the important new techniques that are covered are micro-thermal analysis, pulsed thermal analysis, fast-scanning calorimetery and the use of quartz-crystal microbalances. There are detailed reviews of heating - stage spectroscopy, the range of electrical techniques available, applications in rheology, catalysis and the study of nanoparticles. The development and application of isoconversional methods of kinetic analysis are described and there are comprehensive chapters on the many facets of thermochemistry and of measuring thermophysical properties. Applications to inorganic and coordination chemistry are reviewed, as are the latest applications in medical and dental sciences, including the importance of polymorphism. The volume concludes with a review of the use and importance of thermal analysis and calorimetry in quality control.



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Thermal Analysis of Pharmaceuticals

By Duncan Q.M. Craig, Mike Reading
Publisher: CRC
Number of Pages: 416
Publication Date: 2006-12-21
Book Description:
As a result of the Process Analytical Technologies (PAT) initiative launched by the U.S. Food and Drug Administration (FDA), analytical development is receiving more attention within the pharmaceutical industry. Illustrating the importance of analytical methodologies,Thermal Analysis of Pharmaceuticals presents reliable and versatile characterization tools for the successful development of pharmaceutical products. It draws attention to the most widely applicable methods and demonstrates how to interpret the associated data.
The book opens with the first three chapters devoted to differential scanning calorimetry (DSC), the most commonly used thermal method. These chapters cover the principles, optimal use, and pharmaceutical applications of the method. Subsequent chapters explore modulated temperature DSC, thermogravimetric analysis, thermal microscopy, microcalorimetry, high sensitivity DSC, dynamic mechanical analysis, and thermally stimulated current, all of which have attracted great interest within the pharmaceutical field. The chapters include theoretical background, measurement optimization, and pharmaceutical applications of each technique.
Exploring important techniques for characterizing the physical structure and properties of pharmaceutical materials, Thermal Analysis of Pharmaceuticals achieves an ideal balance in the depth, relevance, and accessibility of topics presented. The book provides an excellent overview of this key area in pharmaceutical development
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Thermal Analysis of Polymers, Fundamentals and Applications



By Joseph D.Menczel, R. Bruce Prime
Publisher: Wiley
Number of Pages: 696
Publication Date: 2009-04-20
Book Description:
Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background.
Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications
Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation.
Written by experts in the various areas of thermal analysis
Relevant and detailed experiments and examples follow each chapter.
 
Characterisation of Polymers by Thermal Analysis


By W.M. Groenewoud
Publisher: Elsevier Science
Number of Pages: 392
Publication Date: 2001-05-01
Book Description:
Thermal Analysis (TA) has become an indispensable family of analytical techniques in the polymer research. The increased importance of these techniques can be seen as the result of three more or less parallel developments: a tempestuous development of TA measuring techniques in combination with a high degree of automation,
the strongly increased understanding of the underlaying theory and, the increasing knowledge of the relation between the polymers' chemical structure and their physical properties.
These areas are still in their developmental stages, especially the third area. The increasing knowledge of the dependence of physical properties on chemical structure just accentuated more and more the need for accurate thermoanalytical measurements, and this knowledge is very important for the first stages of the development of new polymeric systems. Besides, the contribution of TA remains necessary for the technical and commercial development of such a new polymer system. The use of the various TA techniques in these processes is described in this book in nine chapters, while chapter ten illustrates the information obtained about different polymers during special case studies.
This book illustrates in this way, applications of a wide variety of TA techniques whilst it is written from a materials characterisation rather than from a TA point of view with attention being paid to the chemical structure/physical properties correlations.

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Theory of Calorimetry


By W. Zielenkiewicz, E. Margas
Publisher: Springer
Number of Pages: 200
Publication Date: 2002-07-31
Book Description:
The purpose of this book is to give a comprehensive description of the theoretical fundamentals of calorimetry. The considerations are based on the relations deduced from the laws and general equations of heat exchange theory and steering theory. The calorimeter is described as a physical object of well-defined thermal and dynamic parameters. The mathematical models of calorimeters are formulated. A classification of calorimeters is given. The methods of the determination of heat effects and analysis of the course of heat effects in the calorimeters are presented and discussed.
The book enables the reader to understand the principles of operation of various types of calorimeters. This is the first book to deal with theoretical description of calorimetric systems.

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Thermal Analysis Fundamentals and Applications to Polymer



By:T. Hatakeyama, F. X. Quinn
Publisher: Wiley; 2 edition
Publication date 07 9, 1999
Number of pages190 pages
Book Description
Thermal Analysis Fundamentals and Applications to Polymer Science T. Hatakeyama Otsuma Women's University, Tokyo, Japan F. X. Quinn L'Oréal Recherche Advancée, Aulnay-sous-Bois, France The first edition of this classic book remains one of the very few introductory books covering both theoretical and practical aspects of thermal analysis (TA). This new edition includes a much enlarged section on MDSC, in which the instrument is described and a critical appraisal of the technique presented. Other additions include new sections on rate-controlled TGA, OTTER, and Specific Heat Spectroscopy, and a thoroughly updated section on X-Ray DSC. This very practical book is a must for people who use thermal analysis techniques in their everyday work. "An excellent introductory text" - Review of 1st Edition

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Handbook of Thermal Analysis of Construction Materials



By Ralph M. Paroli, James J. Beaudoin, Ana H. Delgado
Publisher: Noyes Data Corporation/Noyes Publications
Number of Pages: 696
Publication Date: 2002-06-15
This comprehensive book containing essential information on the applicability of thermal analysis techniques to evaluate inorganic and organic materials in construction technology should serve as a useful reference for the scientist, engineer, construction technologist, architect, manufacturer, and user of construction materials, standard-writing bodies, and analytical chemists.
The material scientists at the National Research Council of Canada have established one of the best thermal analysis laboratories in the world. Various types of thermal analysis techniques have been applied successfully to the investigation of inorganic and organic construction materials. These studies have provided important information on the characterization of raw as well as finished materials, quality control, quantitative estimation, interrelationships between physical, chemical, mechanical, and durability characteristics.

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Thermal Analysis of Polymeric Materials



By Bernhard Wunderlich
Publisher: Springer; 1 edition
Publication date 05 31, 2005
Book Description
Thermal Analysis of Polymeric Materials systematically treats macroscopic measurements by thermal analysis and the quantitative link to microscopic, molecular structure and mobility. Reversible and irreversible thermodynamics, kinetics, quantum mechanics, and statistical thermodynamics are the roots of the described thermal analysis. The book aims to broaden readers understanding of materials and the connection of flexible macromolecules (polymers) to small molecules and rigid macromolecules (minerals, salts, and metals). An effort is made to discover how the long, flexible molecules fit into their small phases which are characterized as microphases or nanophases. Their order ranges from amorphous to mesophase-like and crystalline. Ultimately, it is shown that the basic structure-property-processing triangle is connected to the better-known types of molecules and their common macroscopic phases.

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