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Pharmaceutical Drug AnalysisBy
Ashutosh Kar
Publisher
New Age Publications (Academic),India
Number Of Pages: 564
Publication Date: 2005-12-01
ISBN-10 / ASIN: 8122415822
ISBN-13 / EAN: 9788122415827
:gift::gift:
Pharmaceutical Drug AnalysisBy
Ashutosh Kar
Publisher
New Age Publications (Academic),India
Number Of Pages: 564
Publication Date: 2005-12-01
ISBN-10 / ASIN: 8122415822
ISBN-13 / EAN: 9788122415827
Book Description
Pharmaceutical Drug Analysis
During the past two decades, there have been magnificent and significant advances in both analytical instrumentation and computerized data handling devices across the globe. In this specific context the remarkable proliferation of windows-based computer software stretched overwhelmingly towards instrument control, real time data handling abilities and the ultimate usage of Laboratory Information Management Systems (LIMS) are surprisingly noteworthy.
Pharmaceutical Drug Analysis in its present form essentially comprises six parts containing in all 32 well-elaborated chapters predominantly dealing with the set of descriptive analytical methodologies developed to control and assure the quality of the final marketed product; and, therefore, includes both qualitative and quantitative methods of analysis to help in the identification as well as purity of the product.
The main purpose of this textbook is to discuss in an explicit and lucid manner several of the newer methods that now find rather wider application in the domain of pharmaceutical analysis. The basic principle of each technique is critically treated with emphasis on factors that directly affect its proper and judicious application to various analytical problems. An in-depth knowledge of these principles, instrumentations, modus operandi, experimental parameters, and sample preparation procedures in order to optimize the performance procedure of typical assay of pharmaceutical secondary products i.e., dosage forms, calculations etc., along with cognate assays from the Official Compendia have been included profusely. Undergraduate and postgraduate students of pharmaceutical drug analysis, quality assurance chemists, industrial trainees, bulk-drug professionals and those in related disciplines earnestly requiring a substantial fundamental understanding and knowledge of the subject will certainly find this a much needed suitable compilation for reading and reference.
The broad coverage included in each of the selected analytical techniques would render Pharmaceutical Drug Analysis to be an useful source of ideas, inspiration for research, and developing newer practical solutions to problems in the ever expanding field of pharmaceutical analysis.
Pharmaceutical Drug Analysis
During the past two decades, there have been magnificent and significant advances in both analytical instrumentation and computerized data handling devices across the globe. In this specific context the remarkable proliferation of windows-based computer software stretched overwhelmingly towards instrument control, real time data handling abilities and the ultimate usage of Laboratory Information Management Systems (LIMS) are surprisingly noteworthy.
Pharmaceutical Drug Analysis in its present form essentially comprises six parts containing in all 32 well-elaborated chapters predominantly dealing with the set of descriptive analytical methodologies developed to control and assure the quality of the final marketed product; and, therefore, includes both qualitative and quantitative methods of analysis to help in the identification as well as purity of the product.
The main purpose of this textbook is to discuss in an explicit and lucid manner several of the newer methods that now find rather wider application in the domain of pharmaceutical analysis. The basic principle of each technique is critically treated with emphasis on factors that directly affect its proper and judicious application to various analytical problems. An in-depth knowledge of these principles, instrumentations, modus operandi, experimental parameters, and sample preparation procedures in order to optimize the performance procedure of typical assay of pharmaceutical secondary products i.e., dosage forms, calculations etc., along with cognate assays from the Official Compendia have been included profusely. Undergraduate and postgraduate students of pharmaceutical drug analysis, quality assurance chemists, industrial trainees, bulk-drug professionals and those in related disciplines earnestly requiring a substantial fundamental understanding and knowledge of the subject will certainly find this a much needed suitable compilation for reading and reference.
The broad coverage included in each of the selected analytical techniques would render Pharmaceutical Drug Analysis to be an useful source of ideas, inspiration for research, and developing newer practical solutions to problems in the ever expanding field of pharmaceutical analysis.
Contents
Part I: GENERAL ASPECTS
Pharmaceutical Chemicals: Purity and Management Theory and Technique of Quantitative Analysis
Errors in Pharmaceutical Analysis and Statistical Validation
Part II: CHEMICAL METHODS
Titrimetric Methods: Acidimetry and Alkalimetry Aqueous Titrations, Non-Aqueous Titration
Redox Methods Permanganate, Dichromate and Ceric Sulphate Titration Methods, Iodimetric and Iodometric Titrations
Precipitation Methods-Argentometric Methods
Complexometric Methods-Complexometric Analysis
Gravimetric Methods-Gravimetric Analysis
Thermoanalytical Methods-Thermoanalytical Analysis
Miscellaneous Methods-Diazotization
Estimation of Phenols and Related Compounds
Karl Fisher Method for Determination of Water
Tertazolium Assay of Steroids
Part III: ELECTROCHEMICAL METHODS
Potentiometric Methods
Amperometric Methods
Part IV: OPTICAL METHODS
Refractometry
Polarimetry
Nephelometry and Turbidimetry
Ultraviolet and Absorption Methods
Infrared Spectrophotometry
Nuclear Magnetic Resonance Spectroscopy
Emission Spectroscopy
Flame Spectroscopy
Atomic Absorption Spectroscopy
Part V: ASSAY METHODS BASED ON SEPARATION TECHNIQUES
Liquid-Liquid Extraction
Thin Layer Chromatography
(TLC)
Gas-Liquid Chromatography
(GLC)
High Performance Liquid Chromatography
(HPLC)
Size Exclusion Chromatography
Part VI: MISCELLANEOUS METHODS
Radioimmunoassay
Part I: GENERAL ASPECTS
Pharmaceutical Chemicals: Purity and Management Theory and Technique of Quantitative Analysis
Errors in Pharmaceutical Analysis and Statistical Validation
Part II: CHEMICAL METHODS
Titrimetric Methods: Acidimetry and Alkalimetry Aqueous Titrations, Non-Aqueous Titration
Redox Methods Permanganate, Dichromate and Ceric Sulphate Titration Methods, Iodimetric and Iodometric Titrations
Precipitation Methods-Argentometric Methods
Complexometric Methods-Complexometric Analysis
Gravimetric Methods-Gravimetric Analysis
Thermoanalytical Methods-Thermoanalytical Analysis
Miscellaneous Methods-Diazotization
Estimation of Phenols and Related Compounds
Karl Fisher Method for Determination of Water
Tertazolium Assay of Steroids
Part III: ELECTROCHEMICAL METHODS
Potentiometric Methods
Amperometric Methods
Part IV: OPTICAL METHODS
Refractometry
Polarimetry
Nephelometry and Turbidimetry
Ultraviolet and Absorption Methods
Infrared Spectrophotometry
Nuclear Magnetic Resonance Spectroscopy
Emission Spectroscopy
Flame Spectroscopy
Atomic Absorption Spectroscopy
Part V: ASSAY METHODS BASED ON SEPARATION TECHNIQUES
Liquid-Liquid Extraction
Thin Layer Chromatography
(TLC)
Gas-Liquid Chromatography
(GLC)
High Performance Liquid Chromatography
(HPLC)
Size Exclusion Chromatography
Part VI: MISCELLANEOUS METHODS
Radioimmunoassay
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