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Spectroscopic Properties of Inorganic and Organometallic
CompoundsVolume 38
:gift::gift:
Spectroscopic Properties of Inorganic and Organometallic
CompoundsVolume 38
A Review of the Literature Published up to Late 2004
Editor
G. Davidson, Formerly School of Chemistry, University of Nottingham, UK
Editor
G. Davidson, Formerly School of Chemistry, University of Nottingham, UK
Authors
K.B. Dillon, University of Durham, UK
D.W.H. Rankin, University of Edinburgh, UK
H.E. Robertson, University of Edinburgh, UK
ISBN-10: 0-85404-451-5
ISBN-13: 978-0-85404-451-1
ISSN 0584-8555
The Royal Society of Chemistry 2006
K.B. Dillon, University of Durham, UK
D.W.H. Rankin, University of Edinburgh, UK
H.E. Robertson, University of Edinburgh, UK
ISBN-10: 0-85404-451-5
ISBN-13: 978-0-85404-451-1
ISSN 0584-8555
The Royal Society of Chemistry 2006
Contents
NMR Spectroscopy in the Liquid and Gas Phases
G. Davidson
1 Introduction
2 Stereochemistry
2.1 Compounds of Group 1
2.2 Compounds of Group 2
2.3 Compounds of Group 3 (Yttrium, Lanthanides,
Actinides)
2.4 Compounds of Group 4
2.5 Compounds of Group 5
2.6 Compounds of Group 6
2.7 Compounds of Group 7
2.8 Compounds of Group 8
2.9 Compounds of Group 9
2.10 Compounds of Group 10
2.11 Compounds of Group 11
2.12 Compounds of Group 12
2.13 Compounds of Group 13
2.14 Compounds of Group 14
2.15 Compounds of Group 15
2.16 Compounds of Group 16
2.17 Compounds of Group 17
2.18 Compounds of Group 18
3 Dynamic Systems
3.1 Fluxional Molecules
3.2 Equilibrium Processes
3.3 Course of Reactions
4 Paramagnetic Complexes
4.1 The Transition Metals
4.2 Lanthanides and Actinides
References
Solid State NMR Spectroscopy
G. Davidson
1 Structure of Solids
1.1 Group 1
1.2 Group 2
1.3 Group 3
1.4 Group 4
1.5 Group 5
1.6 Group 6
1.7 Group 7
1.8 Group 8
1.9 Group 9
1.10 Group 10
1.11 Group 11
1.12 Group 12
1.13 Group 13
1.14 Group 14
1.15 Group 15
1.16 Group 16
1.17 Group 18
2 Motions in Solids
3 Atoms and Molecules Sorbed on to Sol
3.1 Water Sorbed on to Solids
3.2 Other Sorbed Atoms and Molecu
References
Nuclear Quadrupole Resonance Spectroscopy
K.B. Dillon
1 Introduction
2 Main Group Elements
2.1 Group 1 (Lithium-
2.2 Group 13 (Boron-11 and -12, Gallium-69 and -71,
and Indium-115)
2.3 Group 14 (Germanium-73)
2.4 Group 15 (Nitrogen-14, Arsenic-75,
Antimony-121 and -123, and Bismuth-209)
2.5 Group 17 (Chlorine-35 and -37, Bromine-79 and
-81, and Iodine-127)
3 Transition Metals and Lanthanides
3.1 Manganese-55
3.2 Cobalt-59
3.3 Copper-63 and -65
3.4 Lanthanum-139
3.5 Rhenium-187
References
Characteristic Vibrations of Compounds of Main Group Elements
G. Davidson
1 Group 1
2 Group 2
3 Group 13
3.1 Boron
3.2 Aluminium
3.3 Gallium
3.4 Indium
3.5 Thallium
4 Group 14
4.1 Carbon
4.2 Silicon
4.3 Germanium
4.4 Tin
4.5 Lead
5 Group 15
5.1 Nitrogen
5.2 Phosphorus
5.3 Arsenic
5.4 Antimony
5.5 Bismuth
6 Group 16
6.1 Oxygen
6.2 Sulfur
6.3 Selenium
6.4 Tellurium
7 Group 17
8 Group 18
References
Vibrational Spectra of Transition Element Compounds
G. Davidson
1 Scandium, Yttrium and the Lanthanides
2 Titanium, Zirconium and Hafnium
3 Vanadium, Niobium and Tantalum
4 Chromium, Molybdenum and Tungsten
5 Manganese, Technetium and Rhenium
6 Iron, Ruthenium and Osmium
7 Cobalt, Rhodium and Iridium
8 Nickel, Palladium and Platinum
9 Copper, Silver and Gold
10 Zinc, Cadmium and Mercury
11 Actinides
References
Vibrational Spectra of Some Co-ordinated Ligands
G. Davidson
1 Carbon, Silicon, Germanium and Tin Donors
2 Dihydrogen Complexes
3 Boron Donors
4 Carbonyl and Thiocarbonyl Complexes
5 Nitrogen Donors
5.1 Molecular Nitrogen, Azido- and Related Groups
5.2 Amines and Related Ligands
5.3 Ligands Containing >C=N– Groups
5.4 Cyanides, Isocyanides and Related Complexes
5.5 Nitrosyl Complexes
6 Phosphorus and Arsenic Donors
7 Oxygen Donors
7.1 Molecular Oxygen, Peroxo, Aquo and Related
Complexes
7.2 Carboxylate and Related Complexes
7.3 Keto-, Alkoxy-, Ether and Related Complexes
7.4 Ligands Containing O–N, O–P or O–As Bonds
7.5 Ligands Containing O–S or O–Te Bonds
7.6 Ligands Containing O–Cl or O–I Bonds
8 Sulfur and Selenium Donors
9 Potentially Ambident Ligands
9.1 Cyanates, Thio- and Selenocyanates and their
Iso-analogues
9.2 Ligands Containing N and O, N and P or P and O Donor
Atoms
9.3 Ligands Containing N and S, N and Se or P and S Donor
Atoms
9.4 Ligands Containing S and O Donor Atoms
References
Gas-phase Molecular Structures Determined by Electron Diraction
D.W.H. Rankin and H.E. Robertson
1 Introduction
2 Compounds of Elements in Group 2 and 13
3 Compounds of Elements in Group 14
4 Compounds of Elements in Group 15
5 Compounds of Elements in Group 16
6 Compounds of Transition Elements and Lanthanides
References
NMR Spectroscopy in the Liquid and Gas Phases
G. Davidson
1 Introduction
2 Stereochemistry
2.1 Compounds of Group 1
2.2 Compounds of Group 2
2.3 Compounds of Group 3 (Yttrium, Lanthanides,
Actinides)
2.4 Compounds of Group 4
2.5 Compounds of Group 5
2.6 Compounds of Group 6
2.7 Compounds of Group 7
2.8 Compounds of Group 8
2.9 Compounds of Group 9
2.10 Compounds of Group 10
2.11 Compounds of Group 11
2.12 Compounds of Group 12
2.13 Compounds of Group 13
2.14 Compounds of Group 14
2.15 Compounds of Group 15
2.16 Compounds of Group 16
2.17 Compounds of Group 17
2.18 Compounds of Group 18
3 Dynamic Systems
3.1 Fluxional Molecules
3.2 Equilibrium Processes
3.3 Course of Reactions
4 Paramagnetic Complexes
4.1 The Transition Metals
4.2 Lanthanides and Actinides
References
Solid State NMR Spectroscopy
G. Davidson
1 Structure of Solids
1.1 Group 1
1.2 Group 2
1.3 Group 3
1.4 Group 4
1.5 Group 5
1.6 Group 6
1.7 Group 7
1.8 Group 8
1.9 Group 9
1.10 Group 10
1.11 Group 11
1.12 Group 12
1.13 Group 13
1.14 Group 14
1.15 Group 15
1.16 Group 16
1.17 Group 18
2 Motions in Solids
3 Atoms and Molecules Sorbed on to Sol
3.1 Water Sorbed on to Solids
3.2 Other Sorbed Atoms and Molecu
References
Nuclear Quadrupole Resonance Spectroscopy
K.B. Dillon
1 Introduction
2 Main Group Elements
2.1 Group 1 (Lithium-
2.2 Group 13 (Boron-11 and -12, Gallium-69 and -71,
and Indium-115)
2.3 Group 14 (Germanium-73)
2.4 Group 15 (Nitrogen-14, Arsenic-75,
Antimony-121 and -123, and Bismuth-209)
2.5 Group 17 (Chlorine-35 and -37, Bromine-79 and
-81, and Iodine-127)
3 Transition Metals and Lanthanides
3.1 Manganese-55
3.2 Cobalt-59
3.3 Copper-63 and -65
3.4 Lanthanum-139
3.5 Rhenium-187
References
Characteristic Vibrations of Compounds of Main Group Elements
G. Davidson
1 Group 1
2 Group 2
3 Group 13
3.1 Boron
3.2 Aluminium
3.3 Gallium
3.4 Indium
3.5 Thallium
4 Group 14
4.1 Carbon
4.2 Silicon
4.3 Germanium
4.4 Tin
4.5 Lead
5 Group 15
5.1 Nitrogen
5.2 Phosphorus
5.3 Arsenic
5.4 Antimony
5.5 Bismuth
6 Group 16
6.1 Oxygen
6.2 Sulfur
6.3 Selenium
6.4 Tellurium
7 Group 17
8 Group 18
References
Vibrational Spectra of Transition Element Compounds
G. Davidson
1 Scandium, Yttrium and the Lanthanides
2 Titanium, Zirconium and Hafnium
3 Vanadium, Niobium and Tantalum
4 Chromium, Molybdenum and Tungsten
5 Manganese, Technetium and Rhenium
6 Iron, Ruthenium and Osmium
7 Cobalt, Rhodium and Iridium
8 Nickel, Palladium and Platinum
9 Copper, Silver and Gold
10 Zinc, Cadmium and Mercury
11 Actinides
References
Vibrational Spectra of Some Co-ordinated Ligands
G. Davidson
1 Carbon, Silicon, Germanium and Tin Donors
2 Dihydrogen Complexes
3 Boron Donors
4 Carbonyl and Thiocarbonyl Complexes
5 Nitrogen Donors
5.1 Molecular Nitrogen, Azido- and Related Groups
5.2 Amines and Related Ligands
5.3 Ligands Containing >C=N– Groups
5.4 Cyanides, Isocyanides and Related Complexes
5.5 Nitrosyl Complexes
6 Phosphorus and Arsenic Donors
7 Oxygen Donors
7.1 Molecular Oxygen, Peroxo, Aquo and Related
Complexes
7.2 Carboxylate and Related Complexes
7.3 Keto-, Alkoxy-, Ether and Related Complexes
7.4 Ligands Containing O–N, O–P or O–As Bonds
7.5 Ligands Containing O–S or O–Te Bonds
7.6 Ligands Containing O–Cl or O–I Bonds
8 Sulfur and Selenium Donors
9 Potentially Ambident Ligands
9.1 Cyanates, Thio- and Selenocyanates and their
Iso-analogues
9.2 Ligands Containing N and O, N and P or P and O Donor
Atoms
9.3 Ligands Containing N and S, N and Se or P and S Donor
Atoms
9.4 Ligands Containing S and O Donor Atoms
References
Gas-phase Molecular Structures Determined by Electron Diraction
D.W.H. Rankin and H.E. Robertson
1 Introduction
2 Compounds of Elements in Group 2 and 13
3 Compounds of Elements in Group 14
4 Compounds of Elements in Group 15
5 Compounds of Elements in Group 16
6 Compounds of Transition Elements and Lanthanides
References
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