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Stereoselective Synthesis: Workbench Edition​

- Houben-weyl, Methods of Organic Chemistry​

Volume E21a-E21f ) 6 Volumes)​


By J. Houben, Theodor Weyl​


​

Description​





  • Publisher: Thieme Medical Publishers



  • [*]Number Of Pages: 6990

    [*]Publication Date: 1997-01
    [*]
    Binding: Hardcover​


English-language volumes) 6 )

Editors​

G. Helmchen, Heidelberg, Germany
R. W. Hoffmann, Marburg, Germany
J. Mulzer, Frankfurt, Germany
E. Schaumann, Clausthal-Zellerfeld, Germany ​

The development of stereoselective methods of organic synthesis has been the major aim of research in organic chemistry for over a decade, both in academia and in industry. This central field of chemistry has now reached a stage of maturity such that a comprehensive, critical survey is called for. At last, Stereoselective Synthesis provides just that - a six-volume set of almost 7000 pages that evaluates the entire literature of stereoselective chemistry.
The principal part of the work is concerned with methods for stereoselective bond formation. Following the general introductory chapters covering principles, nomenclature, separation, and analysis, the chapters on individual synthetic methods are organized by the type of bond that is broken or formed. Common chiral auxiliaries, solvents, reagents, and catalysts are also covered comprehensively.​

Volume E 21a​

Part A. General Aspects​

Nomenclature and Vocabulary of
Organic Stereochemistry,
G. Helmchen​

Basic Principles of EPC Synthesis,
J. Mulzer​

Determination of Enantiomeric
Purity​

Direct Methods, V. Schurig​

Formation of Diastereomers,
W. Lindner, G. Uray​

Determination of Absolute and
Relative Configuration​

. Nuclear Magnetic Resonance
Methods )Relative Configuration),
H. Duddeck​


x ray ​

and Neutron Diffraction
Methods, G. Maas​

. Chemical Methods, P. Welzel​

Chiroptical Methods, J. Gawronski​


Part B. Synthesis of Axially Chiral
Compounds​


Allenes, C. J. Elsevier​


Biaryls, G. Bringmann, R. Walter,
R. Weirich​

Part C​

Synthesis of Chiral Compounds by Bond
Disconnection, H.-J. Gais​

Part D​

Synthesis of Chiral Compounds by Bond
Formation​


Formation of C—C Bonds​

Alkylation Reactions​

Chiral Nucleophiles, H. Ahlbrecht,​

T. Norin, G. Fráter, H.-E. Högberg,​

L.S. Liebeskind, J.S. McCallum,​

P. Fey, W. Hartwig, G. Solladié​


Chiral Electrophiles, D.S. Matteson,
P. Duhamel​


Chiral Additives, J.M. Brown​

Insertion into C—H Bonds, D.F. Taber​

Volume E 21b​


.( Addition to Carbonyl Groups (C=O)​


Sigma-Type Organometallic Compounds,
R.M. Devant, H.-E. Radunz​


Benzyl-Type Organometallic
Compounds, D. Hoppe​

Allyl-Type Organometallic Compounds,
D. Hoppe, W.R. Roush,
E.J. Thomas​

Enolates, M. Braun, L.S. Liebeskind,
J.S. McCallum, W.-D. Fessner​


Azaenolates or Nitronates, P. Fey,
W. Hartwig​

Metalated Sulfoxides or Sulfoximides,
G. Solladié​

Enzyme-Catalyzed Hydrocyanation,
F. Effenberger, T. Ziegler​

( Addition to Imino Groups) (C=N)​

Sigma-Type Organometallic Compounds,
N. Risch, M. Arend​

Allylic and Allenic Organometallic
Compounds, N. Risch, M. Arend​

Enolates and Related Compounds,
N. Risch, M. Arend​


Strecker and Ugi Reactions, H. Kunz​


N-Acyliminium Ion Additions,
W.N. Speckamp, H. de Koning​

Reactions Involving Olefinic Double
Bonds​

Vinylogous Substitution Reactions,
Y. Yamamoto​


Addition to Alpha,Beta-Unsaturated
Carbonyl Compounds (Michael-Type
(Additions,
Y. Yamamoto, S.G. Pyne,
D. Schinzer, B.L. Feringa,
J.F.G.A. Jansen​

Addition to Olefinic Double Bonds;​

Enimines, Nitroalkenes, 4,5-Dihydrooxazoles,
Alpha,Beta-Unsaturated
Sulfones, Sulfoxides and
Sulfoximines, S.G. Pyne​


Volume E 21c​

. Addition of Free Radicals, B. Giese,
T. Göbel, B. Kopping, H. Zipse​

. Addition of Carbenium Ions to
Olefinic Double Bonds and Allylic
Systems, U. Nubbemeyer​

Allylic Substitutions Catalyzed by​

Transition
​
Complexes,​

P. Metz, T. Lübbers​



. Hydroboration of Olefinic Double

Bonds, M. Zaidlewicz​





Addition to Olefinic Double Bonds

Catalyzed by Transition Metals,
P. Eilbracht​





Pericyclic Reactions​



Cycloadditions, J. Jurczak, T. Bauer,

C. Chapuis, D. Craig, M. Cinquini,
F. Cozzi, W. , P. Binger, D. Fox,
B.B. Snider, J. Mattay, R. Conrads,
H.-U. Reißig​





Ene Reaction, J.K. Whitesell​



Volume E 21d​




. Sigmatropic Rearrangements and​



Electrocyclic Reactions, H. Frauenrath,

J. Kallmerten, J.M. Takacs,
L. Pelter​





.Formation of C—H Bonds​




Protonation of Organometallic​



Compounds, Enolates and

Nitronates, S. Hünig​






Radical Reactions, B. Giese,

A. Ghosez, T. Göbel, H. Zipse​





Reduction of Carbonyl Groups

(C=O)​





. Hydrogenation, H. Brunner​



Reduction with Metals, H.M.R. Hoffmann,

A.M. El Khawaga​





Reduction with Metal Hydrides,

A.P. Davis, M.M. Midland, L.A. Morell​





Hydrosilylation and Subsequent

Hydrolysis, A.P. Davis, H. Brunner​





. Reduction with C—H Hydride

Donors, M.M. Midland, L.A. Morell,
K. Krohn​





-Catalyzed and Biomimetic

Reductions, M. Gottwald​





.( Reduction of Imino Groups (C=N),

J. Martens​





Reduction of Olefinic Double Bonds​



Hydrogenation, U. Kazmaier,

J.M. Brown, A. Pfaltz, P.K. Matzinger,
H.G.W. Leuenberger​





Hydroboration and Hydroalumination,

M. Zaidlewicz​





Sigmatropic Rearrangements,

D. Hasselmann​





Formation of C—Hal Bonds,

R. Bohlmann​






Volume E 21e​





Formation of C—O Bonds​



Oxygenation of Enolates, F.A. Davis,

B.-C. Chen​





Hydroboration of Olefinic Double

Bonds Followed by Oxidation,
M. Zaidlewicz​





Hydrosilylation of Olefinic Double

Bonds Followed by Oxidation,
A.P. Davis​





-Dihydroxylation of Olefinic Double

Bonds, C. Scolastico, G. Poli​





. Epoxidation of Olefinic Double

Bonds, R. Schwesinger, J. Willaredt,
T. Bauer, A.C. Oehlschlager​





Cyclization onto Olefinic Double

Bonds Forming Lactones and Ethers,
G. Cardillo, M. Orena, D. Savoia​





Conjugate Addition of O-Nucleophiles,

A. Berkessel​





Microbial Insertion of Oxygen into

C—H Bonds, K. Petzoldt​





Allylic Oxidation with Singlet

Molecular Oxygen, A.G. Griesbeck,
W. Adam​





. Allylic Oxidation with Selenium

Dioxide, W.-D. Woggon​





. Sigmatropic Rearrangements,

K. Ritter​





Formation of C—S Bonds, M. Mikolajczyk,

J. Drabowicz, P. Kielbasinski​





Formation of C—Se or C—Te Bonds,

M. Mikolajczyk, J. Drabowicz,
P. Kielbasinski​





.

Formation of C—N Bonds​





Electrophilic Amination, G. Boche​



. Addition to Olefinic Double Bonds,

G. Cardillo, M. Orena, D. Savoia​





. Conjugate Addition of N-Nucleophiles,

K. Drauz, M. Schäfer,
M. Schwarm​





. Allylic Substitution Catalyzed by

Palladium Complexes, P. Metz​





Allylic Amination, J.K. Whitesell​



. Sigmatropic Rearrangements,

K. Ritter​





Formation of C—P Bonds,

M. Mikolajczyk, J. Drabowicz,
P. Kielbasinski​





. Formation of C—Si Bonds,

M. Mikolajczyk, J. Drabowicz,
P. Kielbasinski​





Formation of C—Sn Bonds,

M. Mikolajczyk, J. Drabowicz,
P. Kielbasinski​





Volume E 21f​



Appendix Survey of Chiral Auxiliaries,

Solvents, Reagents and Catalysts,
R. Herrmann
Author Index
Subject Index ​



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